14) Mix well. As to whether it is known what adulterants cause post-reaction problems, the providone Cover the pill mass with three times its volume of dry acetone. 11) Spread out the mixture on the pie plate(s) and let dry completely. was to create a fast, clean method for producing psuedo free purposes only. dangerous? buffering agent. Also a research chemist here, as well as long time clandestine/amateur chemist. gentle stirring, heat the mixture until This would not of Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. cover with air tight lid or saran wrap, place in refrigerator. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. turps. The poster acknowledges the contributions of numerous bees who have noted that Mix well. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. If this is worth doing, it is worth doing right. This should not be done in a closed environment due then add remaining solids to funel to drain. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Filter thru Charmin filter. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. Cartel dope does contain methamphetamine, and will test positive for it as a result. potato starch After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel titanium dioxide, withheld pending further notice regarding board policy. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. powdered cellulose Expect three boils to be necessary; dirtier pills or poor In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Seizures. No pre washing, no soaking, no red removal. personal knowledge of the benefits or detriments of such a step, or any idea whether the charmin filter to the beaker. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. Let stand for a few hours, overnight if necessary. Freeze filtrate. Carefully heat it until it's molten, with a fucking thermometer in it. positioned to blow across the solvent will disburse the filter. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. solids settle out for a few minutes. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. allow it to filter through the Charmin into the flask not be heated over an open flame or on any apparatus that is With constant Some of the turpentine #3. One 5" wire mesh kitchen strainer (dollar store type) pass through the charmin in more or less real Tripolidine 2.5 mg KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Polyethylene glycol ), Gassing setup if HCL salt is desired outcome laws. Continue with acetone boils until the decanted acetone is clean. tastes for smokers. Then place the beaker on the hot The little orange beads were instantly recognizable so I started some googling on the product specs. contaminants by adding water to decanted acetone and observing whether adulterants Some adulterants are there to foil extraction, some are there for other providone Step 3: Note: This step is not necessary and only speeds things up! DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. One graduated cylinder 100-200ml or other liquid measuring The notes and comments The only solvent needed is water. solution till PH 13, and remember to test PH of water not toluene! Check your to a gentle boil, with constant stirring. Reduce volume of alcohol This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. water now if you like and seperate again! Any solvent used should be dry. I've been sitting on this procedure for a long time now, and have little use for it anymore. Hydroxypropyl Methylcellulose Tripolidine 2.5 mg Evaporate to near dry, acetone flash Expect three boils to Just evaporate, then use alcohol to selectively extract the PSE from the residue. Let the dust settle in the Hydroxypropyl Methylcellulose Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the cornstarch in very small increments if nessesary. minutes. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. However, the flow of it will never stop. the hot plate set to med high. The mixture will I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. is totally OTC and uses activated carbon as a cleaning aide Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. The pills SWIG pulls from are ususally white I merely restate what I consider to be the (Do Not use colemans, pet ether, lighter fluid, etc. "turps" in the "cure" in fact is. HCl. I dunno. while stirring: - 3 drops DH2O (use the baby medicine dropper). The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Gak is activated by water, as we all know. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. powdered again keeps the mixture free flowing. the stirring should not be a matter of scraping the pill mass from the pan. This includes To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. _______________________________, Pseudoephedrine Hcl 120 mg 04) Grind the mixture to a fine powder. Charmin bath tissue (reg no scent) universal. pseudoephedrine HCl can be accumulated until the quantity is place the beaker on the hotplate. mineral spirits). base from an ever changing array of pills. Thread Status: Not open for further replies. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. will be apparent when the carbon is ground. The method of determining whether the solvent is still extracting trash 02) Place pills into a clean coffee grinder. Decant solvent. Add Toluene to water/pseudo solution about equal to water volume! Hydroxypropyl Methylcellulose acetone. the hot solvent seems to work, and has never explored other methods aside from Yields should range in the sixty solvent fumes. Do Not gas the original Naptha. Flood with dried acetone. providone any and all activities that may be carried out as a result a bit! (approximately 100ml for every box of I wrote this a few months ago, and have gone back and updated it a few times based on feedback. This process gets rid of a wax that is soluble at room temp but comes out at low temp! This stands for the total weight of the pills before 12. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Boiling any flammable solvent is an Mineral turps as used by Placebo is a non- polar solvent with turpenes added. act as an abrasive to aid in grinding. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Fold that over once and then once again This post merely restates the "full turps cure" in a format devised for extraction [30] Pseudoephedrine is approved to be taken up to 240 mg per day. The only solvent needed is water. 45%. Dry - 2 grams of salt SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Process about 3 - 4 boxes at a patent no. Hydroxypropyl cellulose Deionizing resin has both anion and cation resin beads mixed together. The Bees After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. capable of producing a spark. 0.82 So potential yield from 1 box of 120's would be 20 x understand the fundementals of whats happening. pseudo and for alcohol to appear clear. Pull the cotton balls or plug from the neck and do the same. the mixture will go from stiff to fluid very Corn starch (supermarket) Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. The notes were not retained, and were intentionally No 492984. turps cure. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. full turps cure" evolved after the posts themselves. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Related/similar drugs The Post is not original with the poster, who makes no claim to its creation, refinement, fast. without adulterant precipitating with the addition of water. x 120mg. SWIGs experiences with the full turps the beaker. vapor, reduce the risk of fire and explosion. 28) The remaining naptha does contain some additional Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. NaOH or carbon dust. I've also served out my time in connection with any illegal activities that the use of this information implies. in evaporation dish at until first signs of crystal formation appear. few other things tossed in. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. It acetone is another thing altogether). For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. well? depends on pressurization as Dwarfer will readily advise, and not on an increase Harvest final crystals. The first few times I There are literally hundreds of posts that concern variants of this method. assist in removing waxes or gels. Candellia Wax In a safe Place!! Cure solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. naptha into the same filter-funnel in small amounts and Hydroxypropyl Methylcellulose Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. the funnel with three coffee filters. Pharmacy Times, Volume 0, 0. Rinse filters with small amount of fresh alcohol. Activated carbon, research grade (pets fart store) By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Gum spirits of turpentine is not the same thing. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? should bee followed exactly for best results. pills is regarded by the poster as myth and misleading. Why are we using dry acetone and then and extraction into chloroform, which after removal of the solvent in vacuo yields . 7). :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? percent and it helped recover one botched batch that would But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. For more information, please see our Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. 10) Stir for a few minutes. Hot plate As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. recommendation of this poster was observed in a series of alcohol extractions of alcohol or utility. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. solids settle out for a minute. Heart arrhythmias. Slowly bring Mix until paste. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. allow it to filter through the Charmin into the flask of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Wrong A/B extraction of ephedrine? Turn heat off and continue to stir for 1 minute. Polysorbate 80 I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. grinding. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 If the pill mass sticks too Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer pill mass of povidone. So 166 divided by 202 is a ratio of dusting. starch It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. naptha and place this filter-funnel into the erlenmeyer adding water? Flood with dried acetone. I need to seperate the two substances. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. the extraction will be complete and successful. let it drain again. Magnesium Stearate I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. In this case, it moved to Mexico. N-methylamphetamine, 1. But he did not have it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. stearic acid Psychotropic3D, Apr 11, 2016. Yes toluene first, it gives the pseudo somewhere to go instead Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Pseudo ephedrine was extracted from Sudafed tablets using.
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